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Inorganic Syntheses

Volume 35, Inorganic Syntheses 35
Wiley-VCH GmbH
ISBN/EAN: 9780471682554
Umbreit-Nr.: 6219655

Sprache: Englisch
Umfang: 224 S.
Format in cm:
Einband: gebundenes Buch

Erschienen am 15.10.2010
Auflage: 1/2010
€ 172,00
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  • Zusatztext

    • The Inorganic Syntheses series provides all users of inorganic substances with detailed and foolproof procedures for the preparation of important and timely compounds. * Includes complete, up-to-date procedures involving important inorganic substances * Contains subject, contributor, and formula indexes

  • Autorenportrait
    • InhaltsangabePreface. Contributors. Dedication. Notice to Contributors and Checkers. Toxic Substances and Laboratory Hazards. Chapter One COMPLEXES OF BULKY ß-DIKETIMINATE LIGANDS. 1. Introduction. 2. ßDiketiminate Precursors HL¯Me,Me3 and TlL¯Me,Me3 (L¯Me,Me3 = 2,4Bis(Mesitylimido)Pentyl). 3. ßDiketiminate Precursors L¯Me,iPr2H, [¯LMe,iPr2Li]x, and [L¯tBu,iPr2K]x (L¯Me,iPr2 = 2,4Bis(2,6Diisopropylphenylimido)Pentyl; L¯tBu,iPr2 = 2,2,6,6 Tetramethyl3,5Bis(2,6Diisopropylphenylimido)Heptyl). 4. ßDiketiminate Precursors L¯tBu,iPr2H and L¯tBu,iPr2Li(THF) (L¯tBu,iPr2=2,2,6,6Tetramethyl3,5 Bis(2,6Diisopropylphenylimido)Heptyl). 5. Scandium Trichloride Tris(Tetrahydrofuran) and ß-Diketiminate-Supported Scandium Chloride Complexes. 6. ßDiketiminateSupported Titanium and Vanadium Dichloride Complexes. 7. ßDiketiminateSupported Vanadium and Chromium Chloride Complexes. 8. ßDiketiminateSupported Manganese and Zinc Complexes. 9. Iron 2,4Bis(2,6Diisopropylphenylimido)Pentyl Chloride (L¯Me,iPr2FeCl). 10. Iron 2,2,6,6-Tetramethyl-3,5-Bis-(2,6-Diisopropylphenylimido)Heptyl Chloride (L¯tBu,iPr2FeCl). 11. Cobalt 2,2,6,6-Tetramethyl-3,5-Bis-(2,6-Diisopropylphenylimido) Heptyl Chloride (L¯tBu,iPr2CoCl). 12. ßDiketiminateSupported Nickel(II) and Nickel(I) Complexes of L¯Me,Me3 (L¯Me,Me3 = 2,4Bis(Mesitylimido)Pentyl). 13. Nickel 2,4-Bis-(2,6-Diisopropylphenylimido)Pentyl Chloride Dimer, [L¯Me,iPr2Ni(µ-Cl)]2. 14. Bis[Copper 2,4-Bis-(2,4,6-Trimethylphenylimido)Pentyl] Toluene, (L¯Me,Me3Cu)2(µ-n²:n²-C7H8). 15. Copper 2,4-Bis-(2,6-Diisopropylphenylimido)Pentyl Chloride (L¯Me,iPr2CuCl). Chapter Two BORON CLUSTER COMPOUNDS. 16. Salts of Dodecamethylcarba-closo-Dodecaborate(--) Anion, CB11Me12, and the Radical Dodecamethylcarba-closo-Dodecaboranyl, CB11Me12. 17. Cesium Dodecahydroxy-closo-Dodecaborate, Cs2[B12(OH)12]. Chapter Three COORDINATION COMPOUNDS. 18. Pentaaquanitrosylchromium Sulfate. 19. The Tetradentate Bispidine Ligand Dimethyl-(3,7-Dimethyl-9-oxo-2,4-bis(2-pyridyl)-3,7-Diazabicyclo[3.3.1]nonane)-1, 5-dicarboxylate and Its Copper(ll) Complex. 20. Tris(2Picolinyl)Methane and Its Copper(I) Complex. Chapter Four CARBENE LIGANDS AND COMPLEXES. 21. 1,3DialkylImidazole2Ylidenes. 22. A Chelating Rhodium N-Heterocyclic Carbene Complex by Transmetallation from a Silver-NHC Intermediate. 23. Rhodium and Iridium N-Heterocyclic Carbene Complexes from Imidazolium Carboxylates. Chapter Five FUNCTIONAL LIGANDS AND COMPLEXES. 24. NtertButyl orthoAminophenol, orthoIminoquinone, and a Zirconium(IV) bis(Aminophenolate) Complex. 25. Synthesis of the Water-Soluble Bidentate (P, N) Ligand PTN(Me) (PTN(Me) = 7-Phospha-3-methyl-1,3,5-triazabicyclo[3.3.1]nonane). 26. Synthesis of Metal-Organic Frameworks: MOF-5 and MOF-177. Chapter Six ORGANOMETALLIC REAGENTS. 27. Tricarbonyl 1,3,5-Trimethyl-1,3,5-Triazacyclohexane Complexes of Chromium(0), Molybdenum(0), and Tungsten(0) [M(CO)3(Me3TACH) (M = Cr, Mo, W)]. 28. Manganese Tricarbonyl Transfer (MTT) Agents. 29. Bis(1,5Cyclooctadiene)Nickel(0). 30. Sodium (n¯5-Cyclopentadienyl)Tris(Dimethylphosphito-P) Cobaltate(III), Na[(C5H5)Co{P(O)(OMe)2}3]. Chapter Seven BIO-INSPIRED IRON AND NICKEL COMPLEXES. 31. IronCyanocarbonyl Complexes [PPN][Fe(CO)4(CN)] and [PPN][FeBr(CO)3(CN)2]. 32. Nickel Complexes of Bis(Diethylphosphinomethyl) Methylamine. 33. Monomeric Iron(II) Complexes Having Two Sterically Hindered Arylthiolates. 34 (1,3Propanedithiolato)Hexacarbonyldiiron and Cyanide Derivatives. Chapter Eight RUTHENIUM COMPLEXES. 35. Ruthenium(II)-Chlorido Complexes of Dimethylsulfoxide. 36. Synthesis of Chloride-Free Ruthenium(II) Hexaaqua Tosylate, [Ru(H2O)6]tos2. 37. Basic Ruthenium Acetate and Mixed Valence Derivatives. 38. DiµChloro(Ethylbenzoate)Diruthenium(II), [(n¯6etb)RuCl2]2. Chapter Nine IRIDIUM COMPLEXES. 39. The Diphosphine tfepma an